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Beilstein J. Org. Chem. 2021, 17, 224–228, doi:10.3762/bjoc.17.22
Graphical Abstract
Scheme 1: Biphenyl-derived mycotoxins.
Scheme 2: Synthesis of arylboronates 6. Conditions: a) TBSCl, DMAP, imidazole, DMF, 50 °C, 4 h (96%); b) NBS,...
Scheme 3: Synthesis of aryl bromides 9. Conditions: f) BBr3, −78 °C to rt, 18 h (71%); g) R = TBS: TBSCl, DMA...
Scheme 4: Final steps in the synthesis of biaryl 1. Conditions: h) Pd(OAc)2, SPhos, Cs2CO3, dioxane/H2O 7:1, ...
Beilstein J. Org. Chem. 2013, 9, 1572–1577, doi:10.3762/bjoc.9.179
Scheme 1: Imidate hydrochloride synthesis discovered by Pinner and Klein [1,2].
Scheme 2: Mechanism of the Pinner reaction.
Scheme 3: Transformations of imidate hydrochlorides.
Scheme 4: Reaction used for optimizations.
Scheme 5: Plausible mechanism of the Lewis acid-promoted Pinner reaction.
Scheme 6: Synthesis of monaspilosin.
Scheme 7: Proposed mechanism of the trimethylsilyl triflate-promoted Ritter reaction.